Synthesis of AI₂O₃-Y₂O₃ Powders from Suspensions with a Spray Drying Technique | Vestnik Tomskogo gosudarstvennogo universiteta. Chimia – Tomsk State University Journal of Chemistry. 2022. № 28. DOI: 10.17223/24135542/28/4

Synthesis of AI₂O₃-Y₂O₃ Powders from Suspensions with a Spray Drying Technique

This work shows the possibility of obtaining AI₂O₃-Y₂O₃ powders synthesized by nano spray drying. The different methods like thermogravimetry, differential scanning calorimetry, X-ray analysis, BET and scanning electron microscopy were used to investigate the obtained powders. The processes of linear shrinkage of samples during thermal and compression consolidation were studied with the use of spark plasma sintering technology. A comparative analysis of powders obtained with the use nanospray drying technique and reverse co-precipitation deposition was carried out. The results showed that the powder with content of 96 vol.% Y₃AI₅O₁₂ can be obtained by nanospray drying technique by calcining the precursor at a temperature of 1100 °C for 10 minutes. Contribution of the authors: the authors contributed equally to this article. The authors declare no conflicts of interests.

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Keywords

chemical synthesis, nanospray drying, reverse co-precipitation, thermogravimetric analysis, spark plasma sintering

Authors

Name	Organization	E-mail
Paygin Vladimir D.	Tomsk Polytechnic University	vpaygin@mail.ru
Deulina Daria E.	Tomsk Polytechnic University	ded5@tpu.ru
Ilela Alfa E.	Tomsk Polytechnic University	alfaedison@mail.ru
Lyamina Galina V.	Tomsk Polytechnic University	lyamina@tpu.ru
Dvilis Edgar S.	Tomsk Polytechnic University	dvilis@tpu.ru
Valiev Damir T.	Tomsk Polytechnic University	rubinfc@tpu.ru
Stepanov Sergei A.	Tomsk Polytechnic University	stepanovsa@tpu.ru
Khasanov Oleg L.	Tomsk Polytechnic University	khasanov@tpu.ru
Ditts Alexander A.	Tomsk Polytechnic University	ditts@tpu.ru

Всего: 9

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