Features of forming tin oxide under annealing of nanopowders obtained via pulse laser ablation of metal tin in aqueous media | Izvestiya vuzov. Fizika. 2019. № 8. DOI: 10.17223/00213411/62/8/205

Features of forming tin oxide under annealing of nanopowders obtained via pulse laser ablation of metal tin in aqueous media

Nanocolloids obtained by pulsed laser ablation (Nd: YAG laser, 1064 nm, 7 ns, 150 mJ) of metallic Sn in pure distilled water and water with additions of hydrogen peroxide and nitric acid, were dried and annealed at a temperature of up to 800 ° C. It was shown that the addition of H₂O₂or HNO₃ precursors affects not only the size characteristics and the structure of the initial nanoparticles, but also the formation process and the final characteristics of SnO₂ during annealing. X-ray data shows that in the case of PLA in water and nitric acid solution, the SnO phase contains in the initial particles. However after annealing the sample obtained by ablation in HNO₃, the intermediate orthorhombic phase SnO₂ is formed. Additional studies by Raman spectroscopy and thermal analysis made it possible to determine the presence of tin hydroxide in the initial samples and the formation of intermediate forms of SnOx oxides upon annealing.

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Keywords

оксид олова, импульсная лазерная абляция, наночастицы, кристаллическая структура, отжиг, спектры комбинационного рассеяния, tin oxide, pulsed laser ablation, nanoparticles, crystal structure, annealing, Raman spectra

Authors

Name	Organization	E-mail
Fakhrutdinova E.D.	National Research Tomsk State University	fakhrutdinovaed@gmail.com
Lapin I. N.	National Research Tomsk State University	201kiop@mail.ru
Svetlichnyi V.A.	National Research Tomsk State University	v_svetlichnyi@bk.ru

Всего: 3

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